Reaktion #70115

ord-424cd18c450e45828a8725a8621ee747

Reaktionsgleichung

CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
→
CC[NH+](C)CC.O=S(=O)([O-])C(F)(F)F
diethylmethylammonium trifluoromethanesulfonate

Edukte

CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)CC
diethylmethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturwhile being cooled by liquid nitrogen
  2. 2
    Sonstigethus obtaining a target ionic conductor

Vorschrift

Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08535849B2uspto-grants-2013_09