Reaktion #698341

Reaktionsgleichung

(E)-N,N-Dimethyl-[5-(4-stilbenecarbonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine

hydrogen chloride

→

desired product

(E)-N,N-dimethyl-[5-(4-stilbenecarbonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine hydrochloride

Lösungsmittel

methanol

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenThis mixture was concentrated
2. 2
   Waschenthe resulting solid was washed with diethyl ether

Vorschrift

(E)-N,N-Dimethyl-[5-(4-stilbenecarbonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.208 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. This mixture was concentrated; the resulting solid was washed with diethyl ether to yield the desired product.

Quelle