Reaktion #69039

Reaktionsgleichung

2-Phthalimidoethanesulfonyl chloride

methylamine

→

title compound

2-phthalimidoethane N-methylsulfonamide

Lösungsmittel

water

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe solution obtained this way

Vorschrift

2-Phthalimidoethanesulfonyl chloride (2.0 g) was added portion wise to a solution of 2.0 M methylamine in THF (15 ml) and the solution obtained this way was stirred at room temperature. After 48 hours the reaction mixture was poured in water (50 ml) causing the title compound to precipitate. The product was collected by filtration and recrystallized from EtOH:water, 50:1 to yield: 1.04 g (48%) of the desired product as a solid.

Quelle