Reaktion #6902

Reaktionsgleichung

product

N-ethyl-3-methyl-6-nitroquinolin-2-amine

→

N2-ethyl-3-methylquinoline-2.6-diamine

Lösungsmittel

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe reaction mixture was filtered
2. 2
   Filtrationthrough filter aid
3. 3
   Sonstigethe solvent removed under vacuum
4. 4
   Sonstigeto afford the product, which
5. 5
   Sonstigewas used without further purification

Vorschrift

The product (0.8 g) of Step B and platinum oxide on carbon (˜80 mg) was suspended in methanol. The resulting mixture was hydrogenated at 50 PSI for 1 h. The reaction mixture was filtered through filter aid and the solvent removed under vacuum to afford the product, which was used without further purification.

Quelle