Reaktion #68704
ord-2249a546e80243079730b7f18d3febb6
Reaktionsgleichung
diphenyldiethylphosphonium iodide
hydroxide
→
diphenyldiethylphosphonium hydroxide
Ausbeute 96.0%
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
This 98.45 g of diphenyldiethylphosphonium iodide was then dissolved in water, and converted to the corresponding hydroxide with 270 g of an anionic exchange resin in batch overnight, yielding 271.75 g of a 0.94 M solution of diphenyldiethylphosphonium hydroxide (96% of exchange yield) The diphenyldiethylphosphonium hydroxide was used as SDA source.