Reaktion #684692

Reaktionsgleichung

6-nitroveratraldehyde

allylamine

→

dark oil

Ausbeute 99.9%

6-Nitroveratrylideneallylamine

Ausbeute 99.9%

Lösungsmittel

ethanol

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenThe resulting dark solution was concentrated to dryness in vacuo

Vorschrift

A suspension of 6-nitroveratraldehyde (84 g, 0.4 mole) and ethanol (1200 ml) was refluxed with a solution of allylamine (21 g, 0.44 mole) and ethanol (100 ml) for 1.5 hrs. The resulting dark solution was concentrated to dryness in vacuo leaving 100 g of a dark oil which solidified.

Quelle