Reaktion #682803

ord-df6b992df65442b69da01001d4b20c5f

Reaktionsbedingungen

Temperatur
80°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONThen, was added
  2. 2
    Sonstigea polymerization reaction

Vorschrift

Then, was added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide, followed by stirring at 80° C. to conduct a polymerization reaction. After 114 hours, the same post-treatment as in Example 1 was carried out to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 62% and the conversion rate of acrylonitrile was 64%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 5. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09243100B2uspto-grants-2016_01