Reaktion #67828
ord-6ce4660d92144a9c858bce706b3ccc36
Reaktionsgleichung
3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid
intermediate 1
3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid
hydrazinecarboxylic acid tert-butylester
→
tert-butyl 2-{3-[(2-fluoro-4-iodophenyl)amino]isonicotinoyl}hydrazine-carboxylate
Edukte
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeLC/MS [9.37 min; 473 (M+1)]
Vorschrift
tert-butyl 2-{3-[(2-fluoro-4-iodophenyl)amino]isonicotinoyl}hydrazine-carboxylate was synthesized according to the procedure for General Method 1, outlined above, starting with 3 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 5 mmol of hydrazinecarboxylic acid tert-butylester. LC/MS [9.37 min; 473 (M+1)]