Reaktion #677138

Reaktionsgleichung

Sulfamide

oxetan-3-amine

→

title compound

3-(Sulfamoylamino)oxetane

Lösungsmittel

H2O

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.WAITat 100° C. for another 16 h
2. 2
   SonstigeThe obtained reaction mixture
3. 3
   Temperaturwas cooled to rt
4. 4
   Sonstigefreezedried

Vorschrift

Sulfamide (15.6 mmol) was dissolved in H2O (8 mL), added oxetan-3-amine (6.85 mmol) and stirred at 70° C. for 16 h and then at 100° C. for another 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as white solid. Used without further purification.

Quelle