Reaktion #676209

Reaktionsgleichung

Bromine

1-(1,3-thiazol-2-yl)ethanone

→

2-bromo-1-(1,3-thiazol-2-yl)ethanone

Ausbeute 100.0%

Lösungsmittel

AcOH

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenwas concentrated under reduced pressure

Vorschrift

Bromine (70 μL, 1 mmol) was added to a mixture of 1-(1,3-thiazol-2-yl)ethanone (200 mg, 2 mmol) in AcOH (5 mL). The reaction mixture was stirred at 100° C. for 30 min. and was concentrated under reduced pressure to give 2-bromo-1-(1,3-thiazol-2-yl)ethanone as an oil (100%) used as crude.

Quelle