Reaktion #67543

Reaktionsgleichung

tripeptide

N-(N-(N-(9-fluorenylmethyloxycarbonyl)-glycyl)L-phenylalanyl)glycine

piperidine

→

N-(N-(glycyl)-L-phenylalanyl)glycine

Lösungsmittel

DMF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenthe reaction mixture was concentrated to dryness
2. 2
   SonstigeThe crude material was used for the next step without purification

Vorschrift

Fmoc-protected tripeptide 74 (546 mg, 0.98 mmol) was treated with a 5% v/v solution of piperidine in DMF (5 mL). After stirring for 45 min, the reaction mixture was concentrated to dryness. The crude material was used for the next step without purification.

Quelle