Reaktion #66979

ord-8270844e8c9c4a2aa36d4cea219762d2

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturthe reaction was refluxed overnight
  2. 2
    EinengenThe mixture was concentrated

Vorschrift

To 3-bromo-4-methoxyphenylacetic acid (1.0 g, 4.1 mmol) in MeOH (20 mL) was added HCl (4N in 1,4-dioxane; 5 mL, 20 mmol), and the reaction was refluxed overnight. The mixture was concentrated to give the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08524748B2uspto-grants-2013_09