Reaktion #669052

ord-27087c85a34b4171b41c14f8dcbd6063

Reaktionsgleichung

CCc1c(C(=O)c2cc(C)cc(C)c2)[nH]c(=O)[nH]c1=O
5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione
Cc1ccccc1S(=O)(=O)OCC1CCCC1
(cyclopentyl)-methyl toluenesulfonate
→
CCc1c(C(=O)c2cc(C)cc(C)c2)n(CC2CCCC2)c(=O)[nH]c1=O
titled compound
Ausbeute 56.4%
CCc1c(C(=O)c2cc(C)cc(C)c2)n(CC2CCCC2)c(=O)[nH]c1=O
1-(Cyclopentyl)methyl-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione
Ausbeute 56.4%

Edukte

CCc1c(C(=O)c2cc(C)cc(C)c2)[nH]c(=O)[nH]c1=O
5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione
Cc1ccccc1S(=O)(=O)OCC1CCCC1
(cyclopentyl)-methyl toluenesulfonate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and (cyclopentyl)-methyl toluenesulfonate were reacted by the same method with example 20 to obtain the titled compound. (80 mg)

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05922727uspto-grants-1999_07