Reaktion #6683

Reaktionsgleichung

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

Ausbeute 99.0%

Lösungsmittel

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThen the catalyst was filtered out
2. 2
   Sonstigefiltrate was evaporated to dryness
3. 3
   Sonstigeto give the pure compound in yield of 99%

Vorschrift

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

Quelle