Reaktion #66709

Reaktionsgleichung

1-Methoxy-4-nitro-2-trifluoromethyl-benzene

→

4-Methoxy-3-trifluoromethyl-phenylamine

Ausbeute 100.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe reaction mixture was filtered through celite
2. 2
   Sonstigethe filtrate was evaporated in vacuo

Vorschrift

1-Methoxy-4-nitro-2-trifluoromethyl-benzene (10 g, 45 mmol) was hydrogenated in a Paar apparatus with shaking at 50 psi for 4 hours, with 1 g 10 wt % Pd/C. The reaction mixture was filtered through celite, and the filtrate was evaporated in vacuo to give 8.6 g 4-Methoxy-3-trifluoromethyl-phenylamine, 99%, as a solid.

Quelle