Reaktion #66590

Reaktionsgleichung

Iodomethane

3-((dimethylamino)methyl)-5-methylhexan-2-one

→

title product

Ausbeute 68.4%

(2-Acetyl-4-methyl-pentyl)-trimethyl-ammonium iodide

Ausbeute 68.4%

Lösungsmittel

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtration, and the resulting preciptant was collected by filtration

Vorschrift

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

Quelle