Reaktion #66289

ord-7748fb0ae7824eeb97b2dcf13b52c054

Reaktionsgleichung

CC1(C)OB(c2ccc(C=O)c([N+](=O)[O-])c2)OC1(C)C
2-nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde
Brc1ccccn1
2-bromopyridine
→
O=Cc1ccc(-c2ccccn2)cc1[N+](=O)[O-]
title compound
O=Cc1ccc(-c2ccccn2)cc1[N+](=O)[O-]
2-nitro-4-(pyridin-2-yl)benzaldehyde

Edukte

CC1(C)OB(c2ccc(C=O)c([N+](=O)[O-])c2)OC1(C)C
2-nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde
Brc1ccccn1
2-bromopyridine

Reagenzien

Keine

Lösungsmittel

C1COCCO1
dioxane

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared by the procedure as described in Example 101 (Step C) using 2-nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde and 2-bromopyridine in dioxane (reflux).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08524702B2uspto-grants-2013_09