Reaktion #66199

Reaktionsgleichung

ethyl 9-methoxy-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate

4-fluorobenzoyl chloride

→

title compound

Ethyl 3-(4-Fluorobenzoyl)-9-Methoxy-1,2,3,6-Tetrahydroazepino[4,5-b]Indole-5-Carboxylate

Reaktionsbedingungen

Vorschrift

The title compound was prepared in a manner similar to that described in Example 2A by using ethyl 9-methoxy-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate and 4-fluorobenzoyl chloride; 1H-NMR (CDCl3): δ 10.42 (1H, br s), 7.98 (1H, s), 7.62 (2H, m), 7.28 (1H, m), 7.16 (2H, m), 6.93 (1H, d), 6.88 (1H, dd), 4.24 (4H, m), 3.88 (3H, s), 3.23 (2H, m), 1.23 (3H, t); MS (ES): 409 (MH+).

Quelle