Reaktion #660689

ord-4f4679b9de6c4743b1545c2a5fc6e2b1

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

formanilide method, where formic acid and aniline are used as starting materials to prepare formanilide, which in turn reacts with p-nitro-chlorobenzene in the presence of an acid-binding agent such as potassium carbonate, to produce 4-nitrodiphenylamine, and then, 4-nitrodiphenylamine is reduced by sodium sulfide to form 4-aminodiphenylamine;

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09029603B2uspto-grants-2015_05