Reaktion #655820

ord-be1c48a56c7a4592a8feb930ba554dd9

Reaktionsgleichung

Cc1cccc(C(=O)Cl)c1C
2,3-dimethylbenzoyl chloride
COc1cccc(Cl)c1Cl
2,3-dichloroanisole
[Al+3].[Cl-].[Cl-].[Cl-]
AlCl3
→
COc1ccc(C(=O)c2cccc(C)c2C)c(Cl)c1Cl
2,3-dichloro-4-methoxy-2',3'-dimethylbenzophenone

Edukte

Cc1cccc(C(=O)Cl)c1C
2,3-dimethylbenzoyl chloride
COc1cccc(Cl)c1Cl
2,3-dichloroanisole
[Al+3].[Cl-].[Cl-].[Cl-]
AlCl3

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigereacted

Vorschrift

The Friedel-Crafts procedure of Example 24a is repeated with 33.7 g of 2,3-dimethylbenzoyl chloride, 54 g of 2,3-dichloroanisole and 26.7 AlCl3 being reacted to form 2,3-dichloro-4-methoxy-2',3'-dimethylbenzophenone.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04728662uspto-grants-1988_03