Reaktion #65454

ord-99821b20530c4a8aa920baea154b5d6a

Reaktionsgleichung

CCCCNc1ccccc1
N-butylaniline
O=C(O)C1=COc2ccc(O)cc2O1
7-hydroxy-1,4-benzodioxin-2-carboxylic acid
→
CCCCN(C(=O)C1=COc2ccc(O)cc2O1)c1ccccc1
7-HYDROXY-2-(N-BUTYLANILINOCARBONYL)-I,4-BENZODIOXIN
Ausbeute 78.0%

Edukte

CCCCNc1ccccc1
N-butylaniline
O=C(O)C1=COc2ccc(O)cc2O1
7-hydroxy-1,4-benzodioxin-2-carboxylic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThat compound is obtained in a yield of 78%

Vorschrift

That compound is obtained in a yield of 78% starting from N-butylaniline and 7-hydroxy-1,4-benzodioxin-2-carboxylic acid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05420132uspto-grants-1995_05