Reaktion #65182

Reaktionsgleichung

3-chloro-6-(4-cyanophenyl)-4-(ethoxycarbonyl)-pyridazine

→

3-Chloro-6-(4-cyanophenyl)-pyridazine

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   Extraktionis extracted with ethyl acetate
2. 2
   SonstigeThe organic phase is dried
3. 3
   Sonstigeevaporated down
4. 4
   Sonstigethe residue is chromatographed

Vorschrift

3-chloro-6-(4-cyanophenyl)-4-(ethoxycarbonyl)-pyridazine After the reaction solution has been stirred into water the aqueous phase is extracted with ethyl acetate. The organic phase is dried, evaporated down and the residue is chromatographed. Rf value: 0.37 (silica gel; cyclohexane/ethyl acetate=2:1)

Quelle