Reaktion #64843

Reaktionsgleichung

7-Methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine

bromoacetyl chloride

→

4-bromoacetyl-7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine

Ausbeute 51.5%

Lösungsmittel

triethylamine

Reaktionsbedingungen

Vorschrift

7-Methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (3.0 g), triethylamine (3.1 g) and bromoacetyl chloride (3.2 g) were reacted in the same manner as in Experimental Example 1 to give 4-bromoacetyl-7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (2.5 g).

Quelle