Reaktion #64726

Reaktionsgleichung

2-[bis(4-acetoxyphenyl)methyl]benzoic acid

thionyl chloride

→

desired compound

2-[Bis(4-acetoxyphenyl)methyl]benzoyl chloride

Lösungsmittel

methylene chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeobtained by Reference Example 1
2. 2
   Einengenthe reaction mixture was concentrated under reduced pressure

Vorschrift

In 50 ml of methylene chloride was dissolved 7 g of 2-[bis(4-acetoxyphenyl)methyl]benzoic acid obtained by Reference Example 1, and then 10 ml of thionyl chloride was added dropwise to the solution at room temperature. The reaction mixture was stirred for 2 hours, and the reaction mixture was concentrated under reduced pressure to afford 11.33 g of the desired compound as an oily matter.

Quelle