Reaktion #64587

Reaktionsgleichung

decylmethylamine

isononyl chloride

caustic soda

→

decylisononylmethylamine

Ausbeute 83.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigecontained in a 50 gallon reactor
2. 2
   TemperaturThe organic mixture was cooled
3. 3
   Waschenwashed with water
4. 4
   workup.DISTILLATIONfurther purified by fractional distillation

Vorschrift

A mixture of 300 moles of decylmethylamine, 300 moles of isononyl chloride and 350 moles of 50% caustic soda, contained in a 50 gallon reactor, was heated for 6 hours at a temperature of 190° C. The organic mixture was cooled, washed with water and further purified by fractional distillation. The amination process afforded a yield of 83% decylisononylmethylamine. When nonyl chloride is used instead of isononyl chloride, the product is decylnonylmethylamine.

Quelle