Reaktion #64243

ord-99a05bba987e495ba5a0d1f076287117

Reaktionsgleichung

CCN(C(C)=O)[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine
CCN[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-4-nitroxycyclohexylamine
→
CC(=O)N[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-acetyl-4-nitroxycyclohexylamine
Ausbeute 35.0%

Edukte

CCN(C(C)=O)[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine
CCN[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-4-nitroxycyclohexylamine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine from trans-N-ethyl-4-nitroxycyclohexylamine melting point: 68°-69° C. (ether), yield: 35% of theory.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05411989uspto-grants-1995_05