Reaktion #640563

Reaktionsgleichung

2-aminophenylboronic acid

acryloyl chloride

→

2-Acrylamido-phenylboronic acid

Reaktionsbedingungen

Aufarbeitung

1. 1
   ExtraktionThe product was extracted in acetone
2. 2
   Sonstigedried
3. 3
   Sonstigea rotary evaporator

Vorschrift

2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.

Quelle