Reaktion #63708

ord-dca331bd7c724979a783dd4f38301cb2

Reaktionsgleichung

[Na+].[OH-]
sodium hydroxide
Oc1cccc(Cl)c1
3-chlorophenol
Clc1ccc(Cl)cc1
1,4-dichlorobenzene
CC(=O)N(C)C
dimethylacetamide
Clc1ccc(Oc2cccc(Cl)c2)cc1
3,4'-Dichlorodiphenyl ether

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

80 g (1 mol) of 50% sodium hydroxide are added to a solution of 128.1 g (1 mol) of 3-chlorophenol in 1325 g (9 mol) of 1,4-dichlorobenzene and 27 g (0.3 mol) of dimethylacetamide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04766253uspto-grants-1988_08