Reaktion #63327

Reaktionsgleichung

methyl hydrazine

cyanocarbonimidodithioic acid dimethyl ester

→

title compound

N-Cyano-1-methylhydrazinecarboximidothioic acid, methyl ester

Lösungsmittel

acetonitrile

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resulting solution was evaporated to a gum which
2. 2
   Sonstigewas crystallised from acetonitrile/ether

Vorschrift

A mixture of methyl hydrazine (0.48 ml) and cyanocarbonimidodithioic acid dimethyl ester (1.3 g) in acetonitrile was stirred at 25° for 16 hours. The resulting solution was evaporated to a gum which was crystallised from acetonitrile/ether to give the title compound as colourless granules (210 mg) m.p. 69°-71°.

Quelle