Reaktion #63324

Reaktionsgleichung

3-[3-(1-piperidinylmethyl)phenoxy]propanamine

cyanocarbonimidodithioic acid, dimethyl ester

N'-cyano-N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]carbamimidothioic acid methyl ester

→

N'-Cyano-N-[3-[3-[(dimethylamino)methyl]phenoxy]propyl]carbamimidothioic acid, methyl ester

Reaktionsbedingungen

Vorschrift

Similarly prepared from 3-[3-(1-piperidinylmethyl)phenoxy]propanamine] (10 g) and cyanocarbonimidodithioic acid, dimethyl ester (5.84 g) was N'-cyano-N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]carbamimidothioic acid methyl ester (11.5 g) m.p. 89°-90°.

Quelle