Reaktion #63292

Reaktionsgleichung

iodobenzene

3-methyldiphenylamine

→

3-methylphenyldiphenylamine

Ausbeute 75.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONfollowing charge
2. 2
   SonstigeThe above-identified intended product was obtained as colorless crystals

Vorschrift

The same equipment and conditions as in example I were employed with the following charge: 20.4 grams (0.1 mole) iodobenzene, 27.5 grams (0.15 mole) 3-methyldiphenylamine, 15.0 grams copper powder and 30.0 milliliters of Soltrol® 170. The above-identified intended product was obtained as colorless crystals having a melting point of 69°-70° C. Yield 75%.

Quelle