Reaktion #63175

ord-826f5868f42c4a62aa69bc4709ccb98b

Reaktionsgleichung

c1ccc2[nH]nnc2c1
benzotriazole
O=[N+]([O-])[O-].[Ag+]
silver nitrate
[Ag].c1ccc2[nH]nnc2c1
silver benzotriazole

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Temperatur
40°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAn excess of salts was precipitated by pH adjustment
  2. 2
    Sonstigeremoved

Vorschrift

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was stirred while maintaining at 40° C. A solution of 17 g of silver nitrate in 100 ml of water was added thereto over 2 minutes. An excess of salts was precipitated by pH adjustment and removed. The dispersion was then adjusted to a pH of 6.3 to obtain 400 g of a silver benzotriazole emulsion.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04764458uspto-grants-1988_08