Reaktion #631702

ord-0ace4a359ecf44dcbe95a408d7a7094d

Reaktionsgleichung

O=C(Cl)Nc1ccccc1
N-phenyl carbamyl chloride
CCN(CC)C(=O)Cl
diethylcarbamyl chloride
O=C(Cl)N(c1ccccc1)c1ccccc1
diphenylcarbamyl chloride
O=C1c2ccccc2C(=O)c2c(O)cccc21
1-hydroxyanthraquinone
CCNC(=O)Cl
ethylcarbamyl chloride
→
NC(=O)Oc1cccc2c1C(=O)c1ccccc1C2=O
1-anthraquinonyl carbamate

Edukte

O=C(Cl)Nc1ccccc1
N-phenyl carbamyl chloride
CCN(CC)C(=O)Cl
diethylcarbamyl chloride
O=C(Cl)N(c1ccccc1)c1ccccc1
diphenylcarbamyl chloride
O=C1c2ccccc2C(=O)c2c(O)cccc21
1-hydroxyanthraquinone
CCNC(=O)Cl
ethylcarbamyl chloride

Reagenzien

Keine

Lösungsmittel

c1ccncc1
pyridine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Employing the same procedure as described in Example 4, diethylcarbamyl chloride, diphenylcarbamyl chloride, ethylcarbamyl chloride and N-methyl, N-phenyl carbamyl chloride were respectively reacted with 1-hydroxyanthraquinone in pyridine to obtain the corresponding 1-anthraquinonyl carbamate derivatives.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04451278uspto-grants-1984_05