Reaktion #62842

ord-d5106581954f4fe4a6f2c2f345dfca3c

Reaktionsgleichung

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CNCCO
N-methylethanolamine
→
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)N(C)CCO
title compound
Ausbeute 92.0%
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)N(C)CCO
N-Methyl-N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolamin
Ausbeute 92.0%

Edukte

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
CNCCO
N-methylethanolamine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 2.4 ml of N-methylethanolamine were used. 6.6 g (yield 92%) of the title compound was obtained as a colorless oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04762829uspto-grants-1988_08