Reaktion #62819

ord-7128870d458547f4ab41ea21bae4d085

Reaktionsgleichung

CC(C(=O)OC1(C)CCCCC1)c1ccc(N)cc1
1-methylcyclohexyl 2-(p-aminophenyl)-propionate
CC(C(=O)OC12CC3CC(CC(C3)C1)C2)c1ccc([N+](=O)[O-])cc1
1-adamantyl 2-(p-nitrophenyl)propionate
→
CC(C(=O)OC12CC3CC(CC(C3)C1)C2)c1ccc(N)cc1
1-adamantyl 2-(p-aminophenyl)propionate
Ausbeute 100.0%

Edukte

CC(C(=O)OC1(C)CCCCC1)c1ccc(N)cc1
1-methylcyclohexyl 2-(p-aminophenyl)-propionate
CC(C(=O)OC12CC3CC(CC(C3)C1)C2)c1ccc([N+](=O)[O-])cc1
1-adamantyl 2-(p-nitrophenyl)propionate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigewere reacted

Vorschrift

Using a method similar to that used in the preparation of 1-methylcyclohexyl 2-(p-aminophenyl)-propionate, 21.4 g of 1-adamantyl 2-(p-nitrophenyl)propionate were reacted to obtain 19.42 g (100% yield) of 1-adamantyl 2-(p-aminophenyl)propionate of a light yellow viscous liquid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04762840uspto-grants-1988_08