Reaktion #62750

Reaktionsgleichung

calcium carbonate

3-(1-bromoethyl)benzophenone

→

3-(1-hydroxyethyl)benzophenone

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resultant reaction solution
2. 2
   Extraktionwas extracted with benzene
3. 3
   Trocknena formed benzene layer was then dried with anhydrous sodium sulfate
4. 4
   workup.DISTILLATIONby distilling off the solvent

Vorschrift

In an autoclave, 100 ml of water and 3.3 g of calcium carbonate and 10 g of 3-(1-bromoethyl)benzophenone were placed, and were then heated at 120° C. for 6 hours. The resultant reaction solution was extracted with benzene, and a formed benzene layer was then dried with anhydrous sodium sulfate, followed by distilling off the solvent. The resultant product had the spectrum data which were identical with those of 3-(1-hydroxyethyl)benzophenone.

Quelle