Reaktion #622396

ord-f7d764affc4d4106900c220bf207b9eb

Reaktionsgleichung

COC(N)=O
methyl carbamate
N#C[S-].[Na+]
NaSCN
COC(N)=O.N#C[S-].[Na+]
methyl carbamate NaSCN
Ausbeute 194.2%

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
50°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

To a round-bottom flask, 13.7 g of purified methyl carbamate and 5 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 50° C. for 50 minutes to obtain 18.7 g of methyl carbamate-NaSCN eutectic mixture.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08858837B2uspto-grants-2014_10