Reaktion #620762

ord-0bd0f8e4689c4c5b8364684eaad4b00f

Reaktionsgleichung

3-aminopropyltrimethoxysilane

$CCOC(=O)/C=C\C(=O)OCC$

diethyl maleate

→

Diethyl N-(3-trimethoxysilylpropyl)aminosuccinate

Edukte

3-aminopropyltrimethoxysilane

$CCOC(=O)/C=C\C(=O)OCC$

diethyl maleate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen

See reaction.notes.procedure_details.

Aufarbeitung

1
workup.ADDITIONan initial charge

Vorschrift

Diethyl N-(3-trimethoxysilylpropyl)aminosuccinate was prepared as follows: 51.0 g of 3-aminopropyltrimethoxysilane (Silquest®A-1110, Momentive Performance Materials Inc., USA) were introduced as an initial charge. With thorough stirring, 49.0 g of diethyl maleate (Fluka Chemie GmbH, Switzerland) were added slowly at room temperature and the mixture was stirred at room temperature for 2 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08853341B2uspto-grants-2014_10