Reaktion #61673

Reaktionsgleichung

2,6-difluoro-nitrobenzene

methylamine

→

(3-fluoro-2-nitro-phenyl)-methyl-amine

Lösungsmittel

THF

Reaktionsbedingungen

Vorschrift

Reaction of 2.0 g (2.6 mmol) 2,6-difluoro-nitrobenzene with a 2 molar solution of methylamine in THF analogously to the process for preparing Intermediate 10a. Red solid. Yield: 1.8 g (86%); mass spectroscopy: [M+H]+=171.

Quelle