Reaktion #616072

Reaktionsgleichung

Et3N

4,4,4-trifluorobutanal

→

Bis(4,4,4-trifluorobutyl)amine

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeprovided a colorless oil which
2. 2
   Sonstigewas used directly in the preparation of Example 129

Vorschrift

Following a procedure analogous to that for the synthesis of Example 106, 4,4,4-trifluorobutan-1-amine, HCl (598 mg, 4.00 mmol), Et3N (550 μL, 4.00 mmol) and 4,4,4-trifluorobutanal (504 mg, 4.00 mmol) provided a colorless oil which was used directly in the preparation of Example 129. MS(ESI+) m/z 192.1 (M+H)+.

Quelle