Reaktion #61305

ord-c1a6ef5f9b154afb800f1d65d49574fc

Reaktionsgleichung

CC(=O)c1ccc(O)cc1O
Resacetophenone
NCC(=O)O
Glycine
→
O=C(O)CN=CCc1ccc(O)cc1O
N-[(2,4-Dihydroxyphenyl)ethylidene]glycine

Edukte

CC(=O)c1ccc(O)cc1O
Resacetophenone
NCC(=O)O
Glycine

Reagenzien

Keine

Lösungsmittel

O
Water
O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONThe mixture of all ingredients
  2. 2
    Temperaturis heated at 90 to 95 C for 2 hours

Vorschrift

Ingredients. (1) Water 97.5 (2) Resacetophenone 1.5 (3) Glycine 1.0. Procedure. The mixture of all ingredients is heated at 90 to 95 C for 2 hours. A solution of N-[(2,4-Dihydroxyphenyl)ethylidene]glycine in water is obtained.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07427690B2uspto-grants-2008_09