Reaktion #6109
ord-be2199f40d44415e9d6c4b76de61d7c9
Reaktionsgleichung
dimethylthiocarbamoyl chloride
2-tri-fluoromethylphenol
potassium hydroxide
→
yellow oil
Ausbeute 89.0%
O-2-trifluoromethylphenyl dimethylthiocarbamate
Ausbeute 89.0%
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
If the procedure described in Preparation XI is followed starting from 3.95 g (24.3.10-3 mol) of 2-tri-fluoromethylphenol, 1.43 g (25.6.10-3 mol) of potassium hydroxide and 3.46 g (28.10-3 mol) of dimethylthiocarbamoyl chloride, 5.37 g (yield: 89%) of a yellow oil are obtained.