Reaktion #60855

ord-3d17fd2184ec4c0da700016a6a5861ac

Reaktionsgleichung

Cc1ccc(S(=O)(=O)C(NC=O)c2cccc(I)c2)cc1
Intermediate 52
Cc1ccc(S(=O)(=O)C(NC=O)c2cccc(I)c2)cc1
{(3-iodophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide
O=Cc1ccc(Br)cc1
4-bromobenzaldehyde
Cc1ccc(S(=O)(=O)C(NC=O)c2ccc(Br)cc2)cc1
title compound
Cc1ccc(S(=O)(=O)C(NC=O)c2ccc(Br)cc2)cc1
{(4-Bromophenyl)[(4-methylphenyl)sulfonyl]methyl}formamide

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared by a similar process to that described for Intermediate 52 but using 4-bromobenzaldehyde in place of 3-iodobenzaldehyde. Solid (31 g, 80%);

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07427616B2uspto-grants-2008_09