Reaktion #60757

ord-b37e47316bad4f80aff51432a3d6aa29

Reaktionsgleichung

O=C=Nc1ccccc1
phenyl isocyanate
[N-]=C=O
isocyanate
NC1=c2ccoc2=NCN1c1cccc(N)c1
4-Amino-3-(3-aminophenyl)furo[2,3-d]pyrimidine
NC1=c2ccoc2=NCN1c1cccc(NC(=O)Nc2ccccc2)c1
4-Amino-3-(3-((phenyl)aminocarbonylamino)phenyl)furo[2,3-d]pyrimidine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe compound was prepared

Vorschrift

The compound was prepared following the procedure described in Example 232(b), using phenyl isocyanate as the isocyanate of choice, and 4-Amino-3-(3-aminophenyl)furo[2,3-d]pyrimidine (10) as the diamine of choice. MS(ES) m/e 346 [M+H]+.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07427623B2uspto-grants-2008_09