Reaktion #60585

Reaktionsgleichung

1-t-butoxycarbonyl-3-piperidinecarboxanilide

hydrochloride

→

3-piperidinecarboxanilide hydrochloride

Ausbeute 55.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationFiltration of the precipitate

Vorschrift

A solution of 1-t-butoxycarbonyl-3-piperidinecarboxanilide (437 mg, 1.43 mmol) and hydrochloride (1 ml, 4.00 mmol, 4N ethyl acetate) was stirred for several hours. Filtration of the precipitate gave 3-piperidinecarboxanilide hydrochloride (187 mg, 55%).

Quelle