Reaktion #60220

Reaktionsgleichung

2-{N-[2-({2-[(6-amino-5-nitro(2-pyridyl))amino]ethyl}amino)-4-(2,4-dichlorophenyl)pyrimidin-5-yl]carbamoyl}benzoic acid

→

2-[2-({2-[(6-amino-5-nitro(2-pyridyl))amino]ethyl}amino)-4-(2,4-dichlorophenyl)pyrimidin-5-yl]isoindoline-1,3-dione

Lösungsmittel

acetic acid

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenconcentrated in vacuo

Vorschrift

1 mmol of 2-{N-[2-({2-[(6-amino-5-nitro(2-pyridyl))amino]ethyl}amino)-4-(2,4-dichlorophenyl)pyrimidin-5-yl]carbamoyl}benzoic acid was heated to 120° C. in glacial acetic acid for four hours and concentrated in vacuo.

Quelle