Reaktion #60199
ord-563adb478c9f459cb0ea45d4f334cec9
Reaktionsgleichung
1-(2,4-dichlorophenyl)-2-pyrazolylethan-1-one
4-methylimidazole
→
1-(2,4-Dichlorophenyl)-2-(4-methylimidazolyl)ethan-1-one
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThe crude residue was purified on silica gel (5% MeOH/CH2Cl2)
- 2Sonstigeto yield a light yellow solid
Vorschrift
Made using the same procedure as for 1-(2,4-dichlorophenyl)-2-pyrazolylethan-1-one except that 4-methylimidazole (3.7 g, 44.8 mmol) was used in place of pyrazole. The crude residue was purified on silica gel (5% MeOH/CH2Cl2) to yield a light yellow solid.