Reaktion #60067

Reaktionsgleichung

2,4-dichlorophenacyl chloride

phthalimide

Cs2CO3

→

2-[2-(2,4-dichlorophenyl)-2-oxoethyl]isoindoline-1,3-dione

Lösungsmittel

DMF

DMF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigepurified by trituration with diethyl ether

Vorschrift

1 mmol of 2,4-dichlorophenacyl chloride in DMF was added drop wise to 2 mmol of phthalimide and 2 mmol of Cs2CO3 in DMF at room temperature for fourteen hours and then purified by trituration with diethyl ether to obtain 2-[2-(2,4-dichlorophenyl)-2-oxoethyl]isoindoline-1,3-dione.

Quelle