Reaktion #599525

ord-0e6d0709aa184d18b64efb881288d4db

Reaktionsgleichung

O=C(O)c1cccc(Cl)c1Cl
2,3-dichlorobenzoic acid
COCCC(CN)c1cnc(C(F)(F)F)nc1
4-methoxy-2-(2-(trifluoromethyl)pyrimidin-5-yl)butan-1-amine
→
COCCC(CNC(=O)c1cccc(Cl)c1Cl)c1cnc(C(F)(F)F)nc1
2,3-dichloro-N-(4-methoxy-2-(2-(trifluoromethyl)pyrimidin-5-yl)butyl)benz amide

Edukte

O=C(O)c1cccc(Cl)c1Cl
2,3-dichlorobenzoic acid
COCCC(CN)c1cnc(C(F)(F)F)nc1
4-methoxy-2-(2-(trifluoromethyl)pyrimidin-5-yl)butan-1-amine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

From 2,3-dichlorobenzoic acid and 4-methoxy-2-(2-(trifluoromethyl)pyrimidin-5-yl)butan-1-amine. LCMS (MH+): m/z=422.0, tR (minutes, Method F)=2.73

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09102591B2uspto-grants-2015_08