Reaktion #59905

Reaktionsgleichung

( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

6,10-dioxaspiro[4.5]dec-8-ylmethanol

→

title compound

Ausbeute 8.1%

2-(((4-(6,10-dioxaspiro[4.5]dec-8-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

Ausbeute 8.1%

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeobtained in the step (21a)

Vorschrift

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 6,10-dioxaspiro[4.5]dec-8-ylmethanol obtained in the step (21a) to obtain the title compound (180 mg, total yield: 8.1%) as a light yellow solid.

Quelle